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The carrier particles received in each zone of the well include nano-sized particles that are chemically unique to that zone. Fines migration has been troublesome during oil and gas production, as well as during many oil and gas recovery operations including, but not necessarily limited to, acidizing, fracturing, gravel packing, secondary and tertiary recovery operations, and the like. The particulate additive, also referred to herein as nano-sized particles or nanoparticles may fixate or flocculate fines, such as clay and non-clay particles to keep or restrict or reduce the fine particles from moving in, for example, a propped hydraulic fracture in a subterranean formation. As defined herein, fines (i.e. formation fines) are naturally occurring particles having particle size less than 37 microns (μm). As discussed in SPE 81017 referred to above, most of the fines that migrate and cause damage have a charge, and most clay particles generally have an overall negative charge. Detecting such nanoparticles is useful in situations where a well has more than one zone, such as sequential multi-stage fracturing treatments in horizontally completed shale or tight gas completions. Nano-sized particles like magnesium oxide (MgO) may be used to fixate formation fines such as clay and quartz in subterranean hydrocarbon formations to inhibit, restrain, or prevent the fines from migrating to near-wellbore regions to damage production of the hydrocarbons. In this non-limiting example, the nano-sized particles, which coat on the proppant particles, may bind or fix the fines to the proppant particles, such as 20/40 mesh ceramic proppants, so that both the formation fines and the nanoparticles remain on the proppant particles and do not travel or are restrained to the point that fine migration damage to the near-wellbore region is minimized. Should for some reason carrier particles placed during a treatment, such as proppant within a fracture hydraulic fracturing, be produced or flow back into the wellbore they may be detected via the composition of the nano-size particulate additive and/or via a traceable taggant that may be incorporated into the body of the nano-size particulate additive, coated thereon, or both. Since the nano-sized particles for each zone may carry a unique taggant and/or may themselves be unique, the zone from which the nanoparticles were produced may be determined. And if the nano-sized particles from one or more of the zones should flow back into the wellbore on produced proppant particles (or other carrier particle), a sample of the produced proppant containing the uniquely-tagged and/or unique nanoparticles may be analyzed to determine the identity of the nanoparticle(s)/taggant(s). For instance, for each zone in the well, fines-fixing nanoparticles are introduced into the zone, where the nano-sized particles may carry a detectable taggant that is unique to that zone and/or the nano-sized particle itself may be unique to that zone.

Some nano-sized particles, also called nanoparticles herein, not only have high surface areas compared to their small sizes, but also have relatively high surface charges that permit them to associate or connect other particles together, including other charged particles, but also other non-charged particles. In one non-limiting embodiment, these associations or connections between the fines and the nano-sized particles are due to electrical attractions and other intermolecular forces or effects. Matters are further complicated if a well has more than one zone. For instance, operations such as fracturing, gravel packing, and frac-packing may fail allowing undesired flow back or production of carrier particles such as proppant or gravel particles into the wellbore from, for example, the hydraulic fracture in the formation. If there is a failure in a dual or multi-zonal well it may be very difficult to determine which zone failed. These types of zones may be formed in a sequence where one zone is hydraulically fractured, and once completed another zone is hydraulically fractured and completed, the pattern repeating until all frac jobs for the particular well are finished. For instance, nanoparticles may be disposed on carrier particles such as proppant, sand, gravel, and the like. Embodiments, however, are not limited to the forgoing example, and zones are not limited to fracture-based zones-they may be characterized by any type of interval, such as without limitation gravel pack and frac-pack based zones. In one non-limiting example, the subterranean formation proximate a wellbore may be treated with more than one fracture treatment, each fracture area corresponding with a zone. The nano-sized particles used to fixate formation fines and inhibit, restrain, or prevent such fines from migrating may also be used to identify a defective zone in a well having more than one zone. In embodiments where the nano-sized particles do not include taggant material, each zone receives proppant carrying nanoparticles with a chemical make-up that is distinct for that zone. One example of a fracture completion system is FRAC-POINT, which is available from Baker Hughes Incorporated. In addition to fines migration being troublesome during oil and gas production and/or recovery operations, one or more of these operations may periodically fail. The nanoparticles may or may not be tagged with a detectable material. As such, the intended treatment may not be effective and the produced proppant or gravel or the like may cause additional damage such as to the equipment. Such zones may be termed “fracture-based zones”.